Materials Center Leoben Uses HA 100 for Precise Material Analysis Under Hydrogen Influence
Case Study
- Customer: Materials Center Leoben Forschung GmbH
- Location: Leoben, Austria
- Industry: Research Institute & Academia, Metals, Contract Testing
- Topic: MCL: Materials and Components Testing Under the Influence of Hydrogen
January 2025
The Materials Center Leoben (MCL) uses the HA 100 servohydraulic testing machine from ZwickRoell for materials testing under hydrogen influence.With an autoclave (up to 400 bar, -50 °C to +150 °C) and high-precision measurement technology, it enables reliable testing of metallic materials.With the possibility to perform any quasi-static, fracture mechanic and dynamic tests on macroscopic test specimens (e.g. LCF , da/dN , J1C / K1C the machine provides crucial data for material development under extreme conditions.The direct current potential drop method (DCPD) is also used to measure the length of cracks.
Materials Center Leoben Forschung GmbH
MCL sets new standards in materials testing
The Materials Center Leoben (MCL) is a leading research institute in materials science, specializing in the development, optimization and characterization of innovative materials for industrial applications. MCL was founded in 1999 as a limited liability company and has established itself as a competent partner to the industry from the very beginning. The owners reflect its strong academic roots: The Montanuniversität Leoben, Joanneum Research, Leoben Holding, the Austrian Academy of Sciences, the Vienna University of Technology and the Graz University of Technology. As a materials and surface competence center, MCL supports its partners in the development of high-performance and sustainable materials, particularly in the fields of microelectronics, mechanical engineering, aerospace and energy technology.
A key area of research is analyzing the hydrogen compatibility of materials. Hydrogen, as an environmentally friendly energy source, can cause damage to the microstructure of materials and thus influence their mechanical properties. MCL is therefore concentrating on research into hydrogen-material interactions and the associated material changes caused by hydrogen exposure. Based on the results obtained, methods for optimizing materials and methods for the safe design of components for hydrogen-rich environments are being developed.
MCL also operates an ISO IEC 17025 accredited testing laboratory with the most important test methods for mechanical testing of metallic materials such as hardness testing, tensile testing, fracture toughness, fatigue crack growth and fatigue testing. MCL also offers solutions in numerical simulation and model-based material development to accurately predict material behavior and make processes more efficient. Failure analyses and material analysis are key to identifying potential weak points at an early stage and increasing the durability of components. Through interdisciplinary expertise and close cooperation with industry and science, the institute contributes significantly to the development of innovative and sustainable material solutions for the future.
ZwickRoell top competences
- Innovative ZwickRoell complete solution in terms of hydrogen (“everything from a single source”) as the most economical overall package.
- Many years of experience, as ZwickRoell machines are already available.
- Carrying out various fracture mechanics tests.
- Proven quality from ZwickRoell machines.
- Strong software and calibration solution (testXpert).
The task
Precise investigation of damage behavior under the influence of hydrogen
MCL Forschung GmbH provides important material data to support both science and industry in the development of materials suitable for hydrogen applications. The focus is on investigating the damage behavior (material changes, crack formation and crack propagation) in various materials, especially in metals, as soon as they come into contact with hydrogen.
Through comprehensive characterization under varying pressure and temperature conditions, MCL simulates real application conditions—for example for manufacturers of hydrogen pipelines and tanks. They investigate how cracks develop, grow, and affect the crack resistance of materials.
The data obtained is crucial for the development of safe, durable materials that meet the requirements of the hydrogen infrastructure. Customers from various industries, such as power generation and transportation, benefit from these findings to improve their products. MCL actively supports the further development and search for innovative solutions in hydrogen technology.
The ZwickRoell solution
Servohydraulic testing machine HA 100
The HA 100 servohydraulic testing machine was built for MCL to characterize materials under the influence of hydrogen. The HA 100 is equipped with an integrated autoclave that allows pressures of up to 400 bar and temperatures from -50 °C to +150 °C. This machine offers precise measurements of force and elongation and also enables precise in-situ measurement of crack elongation using the direct current potential method. A current is passed through the sample and the change in potential as a result of the crack propagation is measured, thus precisely determining the crack extension.
This special equipment allows the MCL to perform quasi-static, fracture mechanics and fatigue tests (HCF, LCF) with a high degree of flexibility in terms of specimen sizes. In order to carry out tests accurately, it is important that all measuring sensors (such as force, notch expansion, strain, but also in-situ crack length measurement) measure reliably and with the highest precision even under extreme conditions (e.g. high pressures, temperatures). We paid special attention to this aspect, e.g. with regard to pressure-compensated high-precision force measurement in both the low and high force range, so that this system also fulfills all standard requirements with regard to the accuracy of these sensors.
For very precise crack length measurements, the direct current potential drop method (DCPD), which has been established at the MCL for many years, can be used in addition to the frequently used compliance method. This ensures very precise, reliable and safe crack length measurement, which is essential for complex fracture mechanics tests (J-R curves and also fatigue crack growth). When equipping the testing machine with software, particular focus was placed on ensuring that the most important standardized test methods for materials testing of metals for tensile tests, fracture toughness measurements, fatigue crack growth and also strain-controlled fatigue tests can be carried out and also evaluated.
Thanks to the specific equipment mentioned above, the HA 100 is a complete solution for both research and development and testing services in hydrogen technology. It thus supports MCL in the development of safe and efficient materials for the future.
The result
Efficient and precise materials testing
Thanks to the HA 100, MCL can now carry out complex mechanical tests under high-pressure hydrogen and other hydrogen gas mixtures depending on the test temperature from -50 °C to 150 °C. This high-precision testing system solution enables MCL to specialize in fracture mechanics under the influence of hydrogen, among other things, while at the same time successfully mastering the challenges associated with the influence of hydrogen.
With around 25 years of experience in the field of materials testing, MCL already has extensive methodological expertise. The MCL also operates an ISO IEC 17025 accredited test laboratory with currently 18 test procedures in the field of mechanical testing, which ensures the provision of high-quality and reliable tests using standardized test procedures. MCL also plans to include hydrogen atmosphere test methods in the accreditation. By using the HA100, MCL now has a competitive advantage. The reason: The many years of experience with standard test procedures can now also be applied immediately in a hydrogen atmosphere, thus increasing the efficiency and cost-effectiveness of the services. MCL can also deliver fast and reliable results and help its customers to develop safer and better performing materials and products. As a result, MCL is ideally positioned to meet the increasing demands of the industry and drive forward the development of innovative materials.
“The combination of high precision and flexibility allows us to carry out even complex tests efficiently and precisely under the influence of hydrogen and to develop innovative material solutions.”
Dr. Stefan Marsoner,
Head of Department Materials & Services, Materials Center Leoben Forschung GmbH.